Microwave-promoted hydrogenation and alkynylation reactions with palladium-loaded multi-walled carbon nanotubes

Jean-Hubert Olivier, Franck Camerel, Raymond Ziessel, Pascal Retailleau, Julien Amadou, Cuong Pham-Huu

Research output: Contribution to journalArticle

25 Citations (Scopus)

Abstract

Multi-walled carbon nanotubes loaded with Pd(0) clusters (average size distribution 9 nm) have been used under microwave irradiation as catalysts in hydrogenation and alkynylation reactions under "eco-friendly" conditions; reduced cinnamic esters and cross-coupled products were obtained in good yields; use of piperidine as the base provided, in a regiospecific process, novel doubly alkynylated compounds unambiguously characterized by NMR correlation experiments and X-ray diffraction.

Original languageEnglish (US)
Pages (from-to)920-924
Number of pages5
JournalNew Journal of Chemistry
Volume32
Issue number6
DOIs
StatePublished - Jun 17 2008
Externally publishedYes

Fingerprint

Carbon Nanotubes
Microwave irradiation
Palladium
Hydrogenation
Carbon nanotubes
Esters
Microwaves
Nuclear magnetic resonance
X ray diffraction
Catalysts
Experiments
piperidine

ASJC Scopus subject areas

  • Catalysis
  • Chemistry(all)
  • Materials Chemistry

Cite this

Microwave-promoted hydrogenation and alkynylation reactions with palladium-loaded multi-walled carbon nanotubes. / Olivier, Jean-Hubert; Camerel, Franck; Ziessel, Raymond; Retailleau, Pascal; Amadou, Julien; Pham-Huu, Cuong.

In: New Journal of Chemistry, Vol. 32, No. 6, 17.06.2008, p. 920-924.

Research output: Contribution to journalArticle

Olivier, Jean-Hubert ; Camerel, Franck ; Ziessel, Raymond ; Retailleau, Pascal ; Amadou, Julien ; Pham-Huu, Cuong. / Microwave-promoted hydrogenation and alkynylation reactions with palladium-loaded multi-walled carbon nanotubes. In: New Journal of Chemistry. 2008 ; Vol. 32, No. 6. pp. 920-924.
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